Electrolytic gold technology: modern process analysis of precious metal purification

2025-05-13

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Gold, as a global hard currency, its purification technology has always been the core issue of the 

precious metal processing industry. As a contemporary mainstream gold refining technology, 

electrolysis is reshaping the industrial pattern of precious metal purification by virtue of its high 

efficiency, environmental protection, high purity and other advantages. In this paper, we will 

analyze the technical principle of electrolytic gold extraction, process characteristics and industry 

applications, to provide practitioners with systematic technical reference.


Electrolytic gold extraction technology principles and 

process framework


The core principle of gold electrolysis is based on electrochemical redox reaction. Through the construction of 

a specific electrolysis system, the gold-containing raw materials in the anode oxidation reaction, the gold element 

in the form of ions into the electrolyte, and then in the cathode surface reduction for high-purity gold deposits. 

The entire process requires precise control of three main elements:


Electrolyte System

Usually, chloroauric acid (HAuCl₄) is used as the main electrolyte, and hydrochloric acid is used as the acidic 

medium, and the proportioning concentration directly affects the ion migration efficiency. The new 

composite electrolyte can improve current efficiency by more than 15% by adding surfactants.


Electrode material selection

The anode mostly adopts titanium-based platinum-plated electrode, which is both conductive and 

corrosion-resistant; the cathode is made of high-purity titanium plate or 316L stainless steel, and 

the surface roughness needs to be controlled at Ra ≤ 0.8 μm, which ensures the uniform 

deposition of gold layer.


Process parameter control

Current density: conventional range 0.5-1.5A/dm², too high to produce dendritic structure.

Temperature gradient: Maintain 45-65℃ range, cooperate with circulating filtration system.

Pole spacing control: dynamically adjust the 3-8cm spacing to prevent short-circuit


Typical process flow decomposition


Raw material pretreatment stage

The gold-containing waste materials (electronic scrap, jewelry trimmings, mine rough gold, etc.) are graded 

and crushed to 80-200 mesh, and then dissolved in nitric acid - aqua regia system, and then initially 

enriched by activated carbon adsorption or solvent extraction. The key point is to control the pH value 

of the dissolving solution in the range of 1.5-2.5 to ensure that the gold ions are fully dissociated.


Electrolysis refining process

Equipped with special electrolysis tank, adopting multi-stage series power supply mode. The anode area is 

loaded with crude gold plates (purity ≥95%), and the cathode area is placed with titanium templates. A 

single electrolysis cycle takes about 48-72 hours, and the thickness of the cathode deposition layer can 

reach 2-3mm, after stripping, more than 99.99% high purity gold is obtained.


Tail liquid treatment system

Innovative use of ion exchange resin + electrodeposition combination process, so that the concentration of 

residual gold ions in the electrolysis waste liquid is reduced to less than 0.1ppm. The recovered precious 

metal dust is returned to the previous process after press-filtering and drying, realizing the closed-loop 

utilization of resources.


Technical Advantages and Industry Applications


Compared with the traditional fire refining, electrolysis has significant advantages:


Purity breakthrough: the purity of finished gold can reach 99.999%, which meets the aerospace-grade 

material standards.

Reduced energy consumption: unit energy consumption is reduced by 40% compared with the thermal 

method, and the cost of gold treatment per ton is reduced by 25%.

Environmental protection upgrade: 80% reduction of exhaust gas emission and zero wastewater discharge.

High degree of automation: PLC control system realizes real-time monitoring of process parameters.

Current technology has penetrated into many fields:


Precious metal regeneration: treatment of gold-plated contacts in waste circuit boards, with a recovery rate of over 99.5%.

Jewelry Finishing: Preparation of ultra-thin gold foil (thickness ≤ 0.1μm) to enhance the value of the jewelry process.

Electronic industry: production of semiconductor bonding alloy wire to ensure the reliability of microelectronic devices.

Financial reserves: industrialized mass production of central bank-grade standard gold ingots.


Process optimization direction and risk avoidance


Despite the obvious advantages of the electrolysis method, the following technical bottlenecks still need to be noted:


Impurity interference: silver, copper and other associated metals are easy to co-deposited in the cathode, the 

need to develop selective deposition of film technology

Equipment corrosion: the impact of strong acid environment on the life of the electrode, is testing ceramic-based 

composite electrode materials

Energy consumption optimization: through pulse electrolysis technology, it is expected to reduce energy 

consumption by 20%.

It is recommended that the production unit establish a three-level quality control system:

① Spectral analysis of raw materials → ② On-line monitoring of electrolysis process → ③ Rapid XRF inspection of finished products.


Industry Development Trend Outlook


With the breakthrough of new nano-electrode materials, the future electrolytic gold extraction technology will show three major trends:


Micro-reactor technology: development of modular electrolysis unit to realize distributed purification

Digital twin system: build process parameter database, dynamically optimize current efficiency through AI algorithm

Green process upgrading: bio-electrolysis technology is expected to replace chemical solvents and promote zero-pollution 

production.

Gold electrolysis technology not only revolutionizes the traditional purification method, but also promotes the transformation 

and upgrading of the precious metal industry chain. For practitioners, mastering the details of the process and continuous 

technological innovation will be the key to grasping the market opportunities. With the enhancement of clean production 

requirements, the intelligent and low-carbon electrolysis system will surely become the new benchmark of the industry.